マツモト　コウゾウ   MATSUMOTO Kouzou   松本 幸三    所属   専修大学  経営学部    職種   教授
言語種別	英語
発行・発表の年月	2020/03
形態種別	速報，短報，研究ノート等（大学，研究機関紀要）
標題	Detailed experimental procedure for the synthesis of 4-fluoropyridine
執筆形態	単著
掲載誌名	Bulletin of the Institute of Natural Sciences Senshu University
掲載区分	国内
出版社・発行元	Institute of Natural Sciences, Senshu University
巻・号・頁	51,pp.63-68
総ページ数	6
概要	The Balz-Schiemann reaction of 4-aminopyridine afforded 4-fluoropyridine (1) in 20% yield, but the special care was required because 1 was unstable under the aqueous conditions. Both the detailed reaction conditions and the appearance of the reaction mixture are reported in detail. The detailed experimental procedure for the isolation of 1 is also presented. Some comments for 1H NMR spectrum of 1 are given.